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Beilstein J. Org. Chem. 2018, 14, 3018–3024, doi:10.3762/bjoc.14.281
Graphical Abstract
Scheme 1: The nucleofugal carbanion unit C escapes from the alkoxides A1M1 or A1M2 (M = metal), generating th...
Scheme 2: Preparation of β-shielded α-lithioacrylonitrile 2Li and its reaction with aldehydes 4–6 to adducts 7...
Scheme 3: Reversible formation of the adduct 13 of adamantan-2-one (11).
Scheme 4: Preparation and cleavage of the adduct 18 of fluoren-9-one (15).
Scheme 5: Proton transfer from dicyclopropyl ketone (19) to 2Li.
Scheme 6: Metal-free release of the carbanion unit in 25 and its seizure by t-BuCH=O (→ 7); Bu = n-butyl.